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10025-67-9

Basic Information
CAS No.: 10025-67-9
Name: Disulfur dichloride
Molecular Structure:
Molecular Structure of 10025-67-9 (Disulfur dichloride)
Formula: Cl2S2
Molecular Weight: 135.04
Synonyms: Chlorosulfane;Dichlorodisulfane;Sulfur chloride;Sulfur monochloride;Sulfur monochloride (S2Cl2);Sulfur subchloride;Thiosulfurous dichloride;Sulfur chloride (S2Cl2);
EINECS: 233-036-2
Density: 1.704 g/cm3
Melting Point: -80 °C(lit.)
Boiling Point: 137.999 °C at 760 mmHg
Flash Point: 118ºC
Solubility: Soluble in benzene, ether, carbon disulfide
Appearance: Light amber to yellowish red oily liquid with choking and irritant stench
Hazard Symbols: ToxicT,CorrosiveC,DangerousN
Risk Codes: 14-20-25-29-35-50
Safety: 26-36/37/39-45-61
Transport Information: UN 3390 6.1/PG 1
PSA: 50.60000
LogP: 2.67540
Synthetic route

molybdenum pentachloride

A

10025-67-9

disulfur dichloride

B

Mo(5+)*3Cl(1-)*S2(2-)=*MoCl3(S2)

Conditions
ConditionsYield
In further solvent(s) (under exclusion of moisture); refluxing in S2Cl2 at 160°C for 5 h; ppt. filtered, washed (CHCl2);A n/a
B 96%
56-23-5

tetrachloromethane

A

10025-67-9

disulfur dichloride

B

75-15-0

carbon disulfide

Conditions
ConditionsYield
byproducts: S(x)Cl2; (N2), bomb reed, heated at 250°C for 24 h; cooled in liquid air in vac., distd.;A 95%
B n/a
byproducts: S(x)Cl2; (N2), bomb reed, heated at 250°C for 15 h; cooled in liquid air in vac., distd.;A 86%
B n/a
byproducts: S(x)Cl2; (N2), bomb reed, heated at 210°C for 8 d; cooled in liquid air in vac., distd.;A 70%
B n/a

barite

7782-50-5

chlorine

A

10025-67-9

disulfur dichloride

B

barium(II) chloride

Conditions
ConditionsYield
With chaircoal with activated chaircoal at 500 °C;A n/a
B 90%
With chaircoal with activated chaircoal at 500 °C;A n/a
B 90%
In melt reduction to BaS in molten BaCl2; blowing chlorine into the melt;
With coal or coke or hydrocarbons at higher temp.;
In melt reduction to BaS in molten BaCl2; blowing chlorine into the melt;
67-66-3

chloroform

A

7647-01-0

hydrogenchloride

B

10025-67-9

disulfur dichloride

C

75-15-0

carbon disulfide

Conditions
ConditionsYield
(N2), bomb reed, heated at 205°C for 60 h; cooled in liquid air in vac. for a week, distd.; Raman spectr.;A n/a
B 80%
C n/a
7704-34-9

sulfur

10025-68-0

diselenium dichloride

A

10025-67-9

disulfur dichloride

B

1087399-32-3

sulfur selenium dichloride

C

10545-99-0

sulfur dichloride

D

10026-03-6

selenium tetrachloride

Conditions
ConditionsYield
In neat (no solvent) heating of equimolar amount in closed tube to 200°C for 6 h;; fractional distillation;;A n/a
B 30%
C n/a
D n/a
In neat (no solvent) heating of equimolar amount in closed tube to 200°C for 6 h;; fractional distillation;;A n/a
B 30%
C n/a
D n/a
In neat (no solvent) heating of equimolar amount in closed tube to 100, 150, 200 or 250°C for 6 h;; fractional distillation;;
In neat (no solvent) heating of equimolar amount in closed tube to 100, 150, 200 or 250°C for 6 h;; fractional distillation;;

arsenic trisulfide

7782-50-5

chlorine

10025-67-9

disulfur dichloride

Conditions
ConditionsYield
In not given room temp.;;
75-18-3

dimethylsulfide

7782-50-5

chlorine

10025-67-9

disulfur dichloride

Conditions
ConditionsYield
In not given
In not given
7704-34-9

sulfur

2696-92-6

nitrosylchloride

10025-67-9

disulfur dichloride

Conditions
ConditionsYield
In further solvent(s) introduction of NOCl into soln. of S in S2Cl2;;
7704-34-9

sulfur

2696-92-6

nitrosylchloride

A

10025-67-9

disulfur dichloride

B

10102-43-9

nitrogen(II) oxide

Conditions
ConditionsYield
In neat (no solvent) introduction of NOCl, 100°C;;
10049-04-4, 25052-55-5

chlorine dioxide

7704-34-9

sulfur

A

10025-67-9

disulfur dichloride

B

7446-09-5

sulfur dioxide

Conditions
ConditionsYield
In neat (no solvent) decompn. under explosion;;

arsenic

7790-99-0

Iodine monochloride

cadmium(II) sulphide

A

10025-67-9

disulfur dichloride

B

7704-34-9

sulfur

C

cadmium(II) iodide

75-15-0

carbon disulfide

865-44-1

iodine trichloride

A

10025-67-9

disulfur dichloride

B

56-23-5

tetrachloromethane

C

sulfur tetrachloride * iodine trichloride

Conditions
ConditionsYield
In neat (no solvent) room temp.;;
75-15-0

carbon disulfide

7782-50-5

chlorine

A

10025-67-9

disulfur dichloride

B

56-23-5

tetrachloromethane

C

463-71-8

thiophosgene

Conditions
ConditionsYield
In gas passing through glowing tube of porcelaine;;
75-15-0

carbon disulfide

7782-50-5

chlorine

10025-67-9

disulfur dichloride

Conditions
ConditionsYield
In neat (no solvent) room temp.;;
In not given0%
75-15-0

carbon disulfide

7782-50-5

chlorine

A

10025-67-9

disulfur dichloride

B

56-23-5

tetrachloromethane

Conditions
ConditionsYield
In neat (no solvent) room temp.; presence of iodine, SbCl5, MoCl5;;

iron sulfide

7782-50-5

chlorine

A

10025-67-9

disulfur dichloride

B

iron(II) chloride

Conditions
ConditionsYield
In neat (no solvent) fast reaction of FeS and Cl2 with evolution of heat;;
7719-09-7

thionyl chloride

cadmium(II) sulphide

A

10025-67-9

disulfur dichloride

B

7446-09-5

sulfur dioxide

C

10108-64-2

cadmium(II) chloride

Conditions
ConditionsYield
In neat (no solvent) reaction of CdS with SOCl2 in a sealed tube at 200 °C;;
In neat (no solvent) reaction of CdS with SOCl2 in a sealed tube at 200 °C;;

potassium chloride

10025-67-9

disulfur dichloride

Conditions
ConditionsYield
With sulfur
With S
With sulfur
7647-14-5

sodium chloride

A

10025-67-9

disulfur dichloride

B

sodium sulfide

Conditions
ConditionsYield
With S In melt reaction during melting;;
With sulfur In melt reaction during melting;;
22205-45-4

copper(I) sulfide

7647-14-5

sodium chloride

A

10025-67-9

disulfur dichloride

B

copper oxychloride

C

7758-99-8

copper(II) sulfate

D

copper dichloride

Conditions
ConditionsYield
With oxygen byproducts: Na2SO4, SO2; information about the react. eqs. in detail and about dependence on temp.;
With oxygen byproducts: Na2SO4, SO2; information about the react. eqs. in detail and about dependence on temp.;

mercury sulfide

7782-50-5

chlorine

A

10025-67-9

disulfur dichloride

B

10545-99-0

sulfur dichloride

C

mercury dichloride

Conditions
ConditionsYield
below 200°C;; almost pure;;A n/a
B n/a
C >99
7719-09-7

thionyl chloride

mercury(II) oxide

A

10025-67-9

disulfur dichloride

B

7791-25-5

sulfuryl dichloride

C

mercury dichloride

Conditions
ConditionsYield
In neat (no solvent) excess of SOCl2;;
In neat (no solvent) excess of SOCl2;;

carnallite

magnesium sulfide

A

10025-67-9

disulfur dichloride

B

7704-34-9

sulfur

C

7439-95-4

magnesium

Conditions
ConditionsYield
Electrolysis;

magnesium sulfide

7786-30-3

magnesium chloride

A

10025-67-9

disulfur dichloride

B

7704-34-9

sulfur

C

7439-95-4

magnesium

Conditions
ConditionsYield
Electrolysis;

lead(II) sulfide

7782-50-5

chlorine

A

10025-67-9

disulfur dichloride

B

lead(II) chloride

Conditions
ConditionsYield
In neat (no solvent) slow reaction of PbS and Cl2 without evolution of heat;;
7719-09-7

thionyl chloride

zinc sulfide

A

10025-67-9

disulfur dichloride

B

7446-09-5

sulfur dioxide

C

7646-85-7

zinc(II) chloride

Conditions
ConditionsYield
In neat (no solvent) reaction last several days at 150 - 200 °C;;

zinc sulfide

copper dichloride

A

10025-67-9

disulfur dichloride

B

22205-45-4

copper(I) sulfide

C

7646-85-7

zinc(II) chloride

Conditions
ConditionsYield
below 150°C;
below 150°C;
7719-09-7

thionyl chloride

phosphorus

A

10025-67-9

disulfur dichloride

B

7446-09-5

sulfur dioxide

C

7719-12-2, 52843-90-0

phosphorus trichloride

Conditions
ConditionsYield
In neat (no solvent) excess SOCl2; 125°C;;
In neat (no solvent) excess SOCl2; 125°C;;
10025-67-9

disulfur dichloride

7440-69-9

bismuth

7787-60-2

bismuth(III) chloride

Conditions
ConditionsYield
heating Bi with S2Cl2 at 138.6°C, 10 hours;;100%
addition of S2Cl2 to Bi;;
addition of S2Cl2 to Bi;;
10025-67-9

disulfur dichloride

88510-23-0

[(C5H5)2Ti(S4C6H10)]

1271-19-8

bis(cyclopentadienyl)titanium dichloride

Conditions
ConditionsYield
In carbon disulfide byproducts: C6H10S6; air atm.; equimolar ratio, stirring, pptn.; filtn. (SiO2);100%
10025-67-9

disulfur dichloride

barium sulfate

barium(II) chloride

Conditions
ConditionsYield
With chlorine heating in a stream of S2Cl2 and chlorine;100%
With chlorine heating in a stream of S2Cl2 and chlorine;100%
10025-67-9

disulfur dichloride

124-40-3

dimethyl amine

928-05-2

N,N'-dithiobis-methanamine

Conditions
ConditionsYield
In diethyl ether at -78 - 20℃; for 1.23333h;99%
With triethylamine In dichloromethane at -20 - 20℃; for 1h;73%
10025-67-9

disulfur dichloride

7704-34-9

sulfur

7439-98-7

molybdenum

molybdenum sulphide chloride

Conditions
ConditionsYield
In neat (no solvent) sealed quartz ampoule (vac.), heating (150°C, 2 h; then 420°C, 40 h); drying (vac., 150°C); elem. anal.;98%
10025-67-9

disulfur dichloride

molybdenum

7704-34-9

sulfur

(92)Mo3S7(4+)*4Cl(1-)=(92)Mo3S7Cl4

Conditions
ConditionsYield
In neat (no solvent) sealed quartz ampoule (vac.), heating (150°C, 2 h; then 420°C, 40 h); drying (vac., 150°C);98%
10025-67-9

disulfur dichloride

molybdenum

7704-34-9

sulfur

(100)Mo3S7(4+)*4Cl(1-)=(100)Mo3S7Cl4

Conditions
ConditionsYield
In neat (no solvent) sealed quartz ampoule (vac.), heating (150°C, 2 h; then 420°C, 40 h); drying (vac., 150°C);98%
10025-67-9

disulfur dichloride

13939-06-5, 199620-15-0

molybdenum hexacarbonyl

2Mo(4+)*6Cl(1-)*S2(2-)*CH2Cl2=Mo2Cl6S2*CH2Cl2

Conditions
ConditionsYield
With CH2Cl2 In dichloromethane byproducts: CO; Irradiation (UV/VIS); standard Schlenk or glove-box techniques, addn. of S2Cl2 to a suspension of Mo(CO)6 in CH2Cl2, heating to reflux, irradiation (150 W W filament bulb), CO evolution, cooling to room temp. after 3.5 h; pptn., filtration, washing (CH2Cl2, Et2O), drying in vac., elem. anal.;98%
10025-67-9

disulfur dichloride

13939-06-5, 199620-15-0

molybdenum hexacarbonyl

molybdenum(V) sulphide trichloride

Conditions
ConditionsYield
In chloroform byproducts: CO, S; 65°C, 0.5 h;97%
In tetrachloromethane byproducts: CO, S; 80°C, 0.5 h;85%
10025-67-9

disulfur dichloride

1605332-69-1

N-2-pyridylimidoyl-2-pyridylamidine

C12H9N5S2(2+)*2Cl(1-)

Conditions
ConditionsYield
In acetonitrile for 16h; Inert atmosphere; Reflux;96%
10025-67-9

disulfur dichloride

363-72-4

Pentafluorobenzene

1043-50-1

pentafluorophenyl sulfide

Conditions
ConditionsYield
With antimony pentafluoride 60°C, 1 h;94%
With SbF5 60°C, 1 h;94%
10025-67-9

disulfur dichloride

bis{N-(N''-morpholinyl-thiocarbonyl)benzamidinato}-nitrido-technetium(V)chloride

dichloro{N-(N''-morpholinyl-thiocarbonyl)benzamidinato}(thionitrosyl)-technetium(II)

Conditions
ConditionsYield
In dichloromethane addn. of S2Cl2 to a soln. of the Tc-complex; stirring (room temp., 2 h).;; filtn., washing (ether), elem. anal.;;94%
10025-67-9

disulfur dichloride

arsenic(III) trioxide

7784-34-1

arsenic trichloride

Conditions
ConditionsYield
In neat (no solvent) byproducts: SO2; heating of dry As2O3 to 95 to 100°C under reflux; addition of S2Cl2 in portions that temp. arise to 120 to 125°C;; distillation; 99% AsCl3;;93%
In neat (no solvent) room temp.;;
In neat (no solvent) byproducts: SO2, S; at 120°C;;
10025-67-9

disulfur dichloride

7704-34-9

sulfur

rhenium(VII) oxide

[Re3(μ3-S)(μ-S2)3Cl6]Cl

Conditions
ConditionsYield
In neat (no solvent)93%
10025-67-9

disulfur dichloride

77933-43-8

TcN(et2dtc)2

dichlorobis(diethyldithiocarbamato)thionitrosyltechnetium(III)

Conditions
ConditionsYield
In dichloromethane S2Cl2 was added to soln. of Tc-complex in CH2Cl2, vol. was reduced, silica-gel column was used, eluted with CH2Cl2 and ethyl acetate/CH2Cl2; collected, recrystd. from ethyl acetate/CH2Cl2; elem. anal.;92%
10025-67-9

disulfur dichloride

28950-34-7

tetrasulfur tetranitride

857244-78-1

thiotrithiazyl chloride

Conditions
ConditionsYield
In tetrachloromethane addn. of 6 fold excess S2Cl2 to S4Cl4 (in CCl4); heating with exclusion of moisture and air; pptn. on boiling; detailed description of apparatus and handling given;; washing (CCl4/N2 atm.); drying (vac.);;90%
In tetrachloromethane boiling for two hours;;
In tetrachloromethane according H. G. Heal, Adv. Inorg. Chem. Radiochim. 15 (1972) 375; boiling CCl4; crystn. on slowly cooling; XRD; DSC; TGA; DTA;
10025-67-9

disulfur dichloride

bis(acetylacetonato)-3-formyl-acetylacetonatochromium(III)

Cr(S2(C(COCH3)2)2)(CH3COC(CHO)COCH3)

Conditions
ConditionsYield
With sodium carbonate In dichloromethane under Ar; to a mixt. of the Cr complex and Na2CO3 in CH2Cl2 was added S2Cl2 in CH2Cl2, stirred for 2 d at 0°C; filtered, solvent was removed under reduced pressure, fractionated withEt2O; elem. anal.;90%
10025-67-9

disulfur dichloride

ammonium hexafluorophosphate

[TcN(Cl)(C12H8N2)2](1+)*Cl(1-)*H2O = [TcN(Cl)(C12H8N2)2]Cl*H2O

[Tc(NS)Cl(C12H8N2)2](1+)*PF6(1-)*H2O = [Tc(NS)Cl(C12H8N2)2]PF6*H2O

Conditions
ConditionsYield
In chloroform refluxed (2 h); cooled; filtered; washed (CHCl3, Et2O); dissolved in water, filtered, NH4PF6 added to induce pptn.; elem. anal.;90%
10025-67-9

disulfur dichloride

109-79-5

1-butanethiol

5943-36-2

dibutyl tetrasulfide

Conditions
ConditionsYield
With triethylamine In dichloromethane at -20 - 20℃; for 1h;90%
10025-67-9

disulfur dichloride

7782-49-2

selenium

20816-12-0

osmium(VIII) oxide

Os2S6Se2Cl8

Conditions
ConditionsYield
In further solvent(s) byproducts: SO2; Oso4 added to 22% soln. of Se in S2Cl2, heated at 60-80°C until SO2 ceased to evolve, sealed, heated at 100°C for 40 h; ppt. septd., filtered under inert atm., washed (S2Cl2, CS2, CCl4), elem.anal.;90%
10025-67-9

disulfur dichloride

7704-34-9

sulfur

7440-33-7

tungsten

25127-53-1

tungsten(VI) sulfide tetrachloride

Conditions
ConditionsYield
In neat (no solvent) heating (2E-4 Torr, 425°C, 48 h), slow cooling;89%
10025-67-9

disulfur dichloride

31340-36-0

lithium perfluoro isopropylideneamide

38005-16-2

bis(hexafluoroisopropylidene amino) disulfane

Conditions
ConditionsYield
25°C 8 h,;89%
25°C 8 h,;89%
10025-67-9

disulfur dichloride

25398-89-4

ReCl2N(n-propyldiphenylphosphine)2

57894-34-5

trichlorobis(n-propyldiphenylphosphine)(thionitrosyl)rhenium

Conditions
ConditionsYield
In dichloromethane N2-atmosphere; addn. of 0.5 equiv. S2Cl2 to Re-complex, stirring (1.5 h); evapn. (1E-2 Torr), crystn. (acetone); elem. anal.;89%
10025-67-9

disulfur dichloride

bromochloronitridotris(diethylphenylphosphine)rhenium(V)

57902-90-6

bromochlorotris(diethylphenylphosphine)(thionitrosyl)rhenium

Conditions
ConditionsYield
In dichloromethane N2-atmosphere; addn. of 0.5 equiv. S2Cl2 to Re-complex, stirring (room temp., 0.5 h); evapn. (1E-2 Torr), recrystn. (1,2-dichloroethane/pentane); elem. anal.;87%
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*Required Fields

Consensus Reports

Reported in EPA TSCA Inventory.

Standards and Recommendations

OSHA PEL: CL 1 ppm
ACGIH TLV: CL 1 ppm
DFG MAK: 1 ppm (5.6 mg/m3)
NIOSH REL: (Sulfur Monochloride) CL 1 ppm

Specification

The Disulfur dichloride, with the CAS registry number 10025-67-9, is also known as Sulfur monochloride. It belongs to the product category of Inorganics. Its EINECS number is 233-036-2. This chemical's molecular formula is Cl2S2 and molecular weight is 135.04. What's more, its systematic name is chlorosulfanyl thiohypochlorite. Pure Disulfur dichloride is a yellow liquid that smokes in air due to reaction with water. It is stable at common pressure and temperature, and it should be sealed and stored in a ventilated and dry place. Moreover, it should be protected from light.

Physical properties of Disulfur dichloride are: (1)ACD/LogP: 1.899; (2)# of Rule of 5 Violations: 0; (3)ACD/LogD (pH 5.5): 1.90; (4)ACD/LogD (pH 7.4): 1.90; (5)ACD/BCF (pH 5.5): 16.34; (6)ACD/BCF (pH 7.4): 16.34; (7)#H bond acceptors: 0; (8)#H bond donors: 0; (9)#Freely Rotating Bonds: 1; (10)Polar Surface Area: 50.6 Å2; (11)Index of Refraction: 1.617; (12)Molar Refractivity: 27.741 cm3; (13)Molar Volume: 79.243 cm3; (14)Polarizability: 10.998×10-24cm3; (15)Surface Tension: 49.65 dyne/cm; (16)Density: 1.704 g/cm3; (17)Boiling Point: 137.999 °C at 760 mmHg; (18)Vapour Pressure: 8.53 mmHg at 25°C.

Preparation: it is synthesized by partial chlorination of elemental sulfur. The reaction takes place at usable rates at room temperature. In the laboratory, chlorine gas is led into a flask containing elemental sulfur. As disulfur dichloride is formed, the contents become a golden yellow liquid. Pure disulfur dichloride is obtained by distilling the yellow-orange liquid over excess elemental sulfur. It also arises from the chlorination of CS2 as in the synthesis of thiophosgene.

S8 + 4 Cl2 → 4 S2Cl2

Uses of Disulfur dichloride: it has been used to introduce C-S bonds. In the presence of AlCl3, Disulfur dichloride reacts with benzene to give diphenyl sulfide. Other uses include manufacturing sulfur dyes, insecticides, synthetic rubbers. It is also used in cold vulcanization of rubbers, as polymerization catalyst for vegetable oils and for hardening soft woods.

S2Cl2 + 2 C6H6 → (C6H5)2S + 2 HCl + 1/8 S8

When you are using this chemical, please be cautious about it as the following:
This chemical will react violently with water, and if contact with water, it will liberate toxic gas. It is harmful by inhalation and is toxic if swallowed. Moreover, it is very toxic to aquatic organisms. This chemical can cause severe burns. In case of contact with eyes, you should rinse immediately with plenty of water and seek medical advice. When using it, you need to wear suitable protective clothing, gloves and eye/face protection. In case of accident or if you feel unwell, you must seek medical advice immediately (show the label where possible). You should avoid releasing it to the environment, and you need to refer to special instructions/safety data sheet.

You can still convert the following datas into molecular structure:
(1)SMILES: ClSSCl
(2)Std. InChI: InChI=1S/Cl2S2/c1-3-4-2
(3)Std. InChIKey: PXJJSXABGXMUSU-UHFFFAOYSA-N

The toxicity data is as follows:  

Organism Test Type Route Reported Dose (Normalized Dose) Effect Source
mouse LC50 inhalation 150ppm (150ppm)   International Polymer Science and Technology. Vol. 3, Pg. 93, 1976.
rat LC50 inhalation 2500mg/m3/4H (2500mg/m3) SENSE ORGANS AND SPECIAL SENSES: CORNEAL DAMAGE: EYE

LUNGS, THORAX, OR RESPIRATION: CYANOSIS

LUNGS, THORAX, OR RESPIRATION: ACUTE PULMONARY EDEMA
International Journal of Toxicology. Vol. 19, Pg. 342, 2000.
rat LD50 oral 132mg/kg (132mg/kg) BEHAVIORAL: GENERAL ANESTHETIC

SKIN AND APPENDAGES (SKIN): HAIR: OTHER

CARDIAC: OTHER CHANGES
International Journal of Toxicology. Vol. 19, Pg. 342, 2000.