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87-63-8

Basic Information
CAS No.: 87-63-8
Name: 2-Chloro-6-methylaniline
Article Data: 19
Molecular Structure:
Molecular Structure of 87-63-8 (2-Chloro-6-methylaniline)
Formula: C7H8ClN
Molecular Weight: 141.6
Synonyms: o-Toluidine,6-chloro- (8CI);(2-Chloro-6-methylphenyl)amine;2-Amino-3-chlorotoluene;
EINECS: 201-759-2
Density: 1.18 g/cm3
Melting Point: 2 °C
Boiling Point: 215 °C at 760 mmHg
Flash Point: 98.9 °C
Solubility: immiscible with water
Appearance: clear yellow to red-brown liquid
Hazard Symbols: HarmfulXn, IrritantXi
Risk Codes: 36/37/38-20/21/22
Safety: 26-36-36/37/39
Transport Information: UN 3429 6.1/PG 3
PSA: 26.02000
LogP: 2.81180
Synthetic route

3-chloro-5-methyl-4-nitroaniline

87-63-8

2-chloro-6-methylaniline

Conditions
ConditionsYield
Stage #1: 3-chloro-5-methyl-4-nitroaniline With sulfuric acid; sodium nitrite In water at 0℃; for 0.5h;
Stage #2: With hypophosphorous acid In water at 0℃; for 3h;
Stage #3: With iron In water at 90℃; for 4h; Reagent/catalyst;
82.5%
69190-56-3

2-bromo-1-chloro-3-methylbenzene

87-63-8

2-chloro-6-methylaniline

Conditions
ConditionsYield
With ammonium hydroxide; L-2-O-methyl-chiro-inositol; copper(II) acetate monohydrate In 1-methyl-pyrrolidin-2-one at 110℃; for 12h;82%
95-53-4

o-toluidine

87-63-8

2-chloro-6-methylaniline

Conditions
ConditionsYield
With N-chloro-succinimide; 1-(3,5-bis(trifluoromethyl)phenyl)-3-((1S,2S)-2-(mesitylselanyl)-2,3-dihydro-1H-inden-1-yl)thiourea In chloroform-d1 at 0℃; for 12h; regioselective reaction;65%
21352-09-0

N-(2-chloro-6-methylphenyl)acetamide

87-63-8

2-chloro-6-methylaniline

Conditions
ConditionsYield
With hydrogenchloride In water at 50 - 55℃; for 7h; Time;61.7%

C9H10ClNO4S

87-63-8

2-chloro-6-methylaniline

Conditions
ConditionsYield
With hydrogenchloride In sulfolane; water at 120℃; for 26h;60%
31656-92-5

1-azido-2-methyl-benzene

87-63-8

2-chloro-6-methylaniline

Conditions
ConditionsYield
With hydrogenchloride
6387-14-0

6-amino-5-chloro-toluene-3-sulfonic acid

87-63-8

2-chloro-6-methylaniline

Conditions
ConditionsYield
With sulfuric acid at 165℃;
With sulfuric acid at 150 - 160℃;
611-22-3

N-(o-tolyl)hydroxylamine

87-63-8

2-chloro-6-methylaniline

Conditions
ConditionsYield
With hydrogenchloride
150545-04-3

N-(2-chloro-6-methylphenyl)pivalamide

87-63-8

2-chloro-6-methylaniline

Conditions
ConditionsYield
With hydrogen bromide for 4.5h; Heating; Yield given;
611-22-3

N-(o-tolyl)hydroxylamine

A

2835-99-6

4-amino-3-methylphenol

B

95-53-4

o-toluidine

C

87-63-8

2-chloro-6-methylaniline

D

95-69-2

4-chloro-2-methylbenzeneamine

Conditions
ConditionsYield
With perchloric acid; sodium perchlorate; sodium chloride In water; acetonitrile at 25℃; Rate constant;
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Chemistry

Molecular Structure of 2-Amino-3-chlorotoluene (CAS NO.87-63-8):

IUPAC Name: 2-chloro-6-methylaniline
CAS Number: 87-63-8
Molecular Formula: C7H8ClN
Molecular Weight: 141.61
EINECS: 201-759-2
Melting Point: 2°C
H bond acceptors: 1
H bond donors: 2
Freely Rotating Bonds: 1
Polar Surface Area: 3.24 Å2
Index of Refraction: 1.585
Molar Refractivity: 40.2 cm3
Molar Volume: 119.9 cm3
Surface Tension: 42.7 dyne/cm
Density: 1.18 g/cm3
Flash Point: 98.9 °C
Enthalpy of Vaporization: 45.13 kJ/mol
Boiling Point: 215 °C at 760 mmHg
Vapour Pressure: 0.151 mmHg at 25°C
Water Solubility: Immiscible
BRN: 774624
Solubility: Immiscible
InChI
InChI=1/C7H8ClN/c1-5-3-2-4-6(8)7(5)9/h2-4H,9H2,1H3
Smiles
c1(c(cccc1Cl)C)N
Product Categories: benzene derivative; Anilines, Aromatic Amines and Nitro Compounds

Toxicity Data With Reference

Organism Test Type Route Reported Dose (Normalized Dose) Effect Source
cat LDLo subcutaneous 200mg/kg (200mg/kg) BEHAVIORAL: CONVULSIONS OR EFFECT ON SEIZURE THRESHOLD

BEHAVIORAL: ATAXIA

LUNGS, THORAX, OR RESPIRATION: OTHER CHANGES
Archiv fuer Hygiene und Bakteriologie. Vol. 110, Pg. 12, 1933.

Consensus Reports

Reported in EPA TSCA Inventory.

Safety Profile

Poison by subcutaneous route. Mutation data reported. When heated to decomposition it emits toxic vapors of NOx and Cl.
Safety Information of  2-Amino-3-chlorotoluene (CAS NO.87-63-8):
Hazard Symbols:Xn 
Risk Codes: 36/37/38-20/21/22
R20/21/22:Harmful by inhalation, in contact with skin and if swallowed. 
R36/37/38:Irritating to eyes, respiratory system and skin.
Safety Statements: 26-36-36/37/39
S26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. 
S36:Wear suitable protective clothing. 
S36/37/39:Wear suitable protective clothing, gloves and eye/face protection.
RIDADR: UN 3429 6.1/PG 3
WGK Germany: 3
RTECS: XU5100000
HazardClass: 6.1
PackingGroup: III

Standards and Recommendations

DOT Classification:  6.1; Label: KEEP AWAY FROM FOOD

Specification

  2-Amino-3-chlorotoluene , with CAS number of 87-63-8, can be called 2-Chloro-6-methylaniline ; 2-Methyl-6-chloroaniline ; 6-Chloro-2-methylaniline ; 6-Chloro-2-toluidine ; 6-Chloro-o-toluidine . It is a clear yellow to red-brown liquid.  2-Amino-3-chlorotoluene (CAS NO.87-63-8) can be used as a medicine, pesticide, dye intermediate.
 

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