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881386-01-2

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Basic Information
CAS No.: 881386-01-2
Name: 2-Piperidinone, 3,3-dichloro-1-(4-nitrophenyl)-
Article Data: 10
Molecular Structure:
Molecular Structure of 881386-01-2 (2-Piperidinone, 3,3-dichloro-1-(4-nitrophenyl)-)
Formula: C11H10Cl2N2O3
Molecular Weight: 289.118
Synonyms: 3,3-dichloro-1-(4-nitrophenyl)-2-piperidinone;QC-8280;2-Piperidinone,3,3-dichloro-1-(4-nitrophenyl);
Density: 1.50
Boiling Point: 520.2±50.0 °C(Predicted)
PSA: 66.13000
LogP: 3.48370
Related products
Synthetic route
38560-30-4

1-(4-nitrophenyl)piperidine-2-one

881386-01-2

3,3-dichloro-1-(4-nitrophenyl)piperidine-2-one

Conditions
ConditionsYield
With phosphorus pentachloride In chlorobenzene at 55℃; for 5h;94.9%
With phosphorus pentachloride In dichloromethane at 40℃; Cooling with ice; Inert atmosphere;93.1%
With phosphorus pentachloride In chloroform for 0.5h; Reflux;88.58%
1575-61-7

5-Chlorovaleroyl chloride

881386-01-2

3,3-dichloro-1-(4-nitrophenyl)piperidine-2-one

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere
2: phosphorus pentachloride / dichloromethane / Reflux
View Scheme
Multi-step reaction with 3 steps
1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 5 - 25 °C / Inert atmosphere
2: sodium hydride / tetrahydrofuran / 10 - 25 °C / Inert atmosphere
3: phosphorus pentachloride / dichloromethane / 40 °C / Cooling with ice; Inert atmosphere
View Scheme
Multi-step reaction with 3 steps
1: trimethylamine / tetrahydrofuran / 0 - 20 °C
2: potassium carbonate; dimethyl sulfoxide / 6 h / 80 °C
3: phosphorus pentachloride / dichloromethane / 5 h / Reflux
View Scheme
100-01-6

4-nitro-aniline

881386-01-2

3,3-dichloro-1-(4-nitrophenyl)piperidine-2-one

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere
2: phosphorus pentachloride / dichloromethane / Reflux
View Scheme
Multi-step reaction with 3 steps
1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 5 - 25 °C / Inert atmosphere
2: sodium hydride / tetrahydrofuran / 10 - 25 °C / Inert atmosphere
3: phosphorus pentachloride / dichloromethane / 40 °C / Cooling with ice; Inert atmosphere
View Scheme
Multi-step reaction with 3 steps
1: trimethylamine / tetrahydrofuran / 0 - 20 °C
2: potassium carbonate; dimethyl sulfoxide / 6 h / 80 °C
3: phosphorus pentachloride / dichloromethane / 5 h / Reflux
View Scheme
1039914-85-6

5-chloro-N-(4-nitrophenyl)pentanamide

881386-01-2

3,3-dichloro-1-(4-nitrophenyl)piperidine-2-one

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: sodium hydride / tetrahydrofuran / 10 - 25 °C / Inert atmosphere
2: phosphorus pentachloride / dichloromethane / 40 °C / Cooling with ice; Inert atmosphere
View Scheme
Multi-step reaction with 2 steps
1: potassium carbonate; dimethyl sulfoxide / 6 h / 80 °C
2: phosphorus pentachloride / dichloromethane / 5 h / Reflux
View Scheme
Multi-step reaction with 2 steps
1: potassium carbonate / dimethyl sulfoxide / 6 h / 80 °C
2: phosphorus pentachloride / dichloromethane / 5 h / Reflux
View Scheme
Multi-step reaction with 2 steps
1: tetrabutylammomium bromide; potassium hydroxide / water; tetrahydrofuran / 0 - 20 °C
2: phosphorus pentachloride / toluene / 1 h / 25 - 80 °C
View Scheme
4509-90-4

5-bromovaleroyl chloride

881386-01-2

3,3-dichloro-1-(4-nitrophenyl)piperidine-2-one

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: pyridine; dmap / tetrahydrofuran / 1 h / 0 - 100 °C
2: phosphorus pentachloride / chloroform / 0.5 h / Reflux
View Scheme
Multi-step reaction with 2 steps
1.1: water; tetrahydrofuran / 1 h / 20 °C / Green chemistry
1.2: 4 h / 20 °C / Green chemistry
2.1: phosphorus pentachloride / chlorobenzene / 2 h / 53 °C / Green chemistry
View Scheme
62-53-3

aniline

881386-01-2

3,3-dichloro-1-(4-nitrophenyl)piperidine-2-one

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1.1: sodium hydroxide; tetrabutylammomium bromide / dichloromethane; water / 1 h / 0 - 5 °C
1.2: 20 °C
2.1: nitric acid; sulfuric acid / 0 - 5 °C
3.1: phosphorus pentachloride / toluene / 1 h / 25 - 80 °C
View Scheme
Multi-step reaction with 4 steps
1: sodium hydroxide; tetrabutylammomium bromide / dichloromethane; water / 1 h / 25 - 30 °C
2: potassium hydroxide / dichloromethane; N,N-dimethyl-formamide / 1 h / 0 - 20 °C / Inert atmosphere
3: nitric acid; sulfuric acid / 0 - 5 °C
4: phosphorus pentachloride / toluene / 1 h / 25 - 80 °C
View Scheme
4789-09-7

1-phenylpiperidin-2-one

881386-01-2

3,3-dichloro-1-(4-nitrophenyl)piperidine-2-one

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: nitric acid; sulfuric acid / 0 - 5 °C
2: phosphorus pentachloride / toluene / 1 h / 25 - 80 °C
View Scheme
91131-23-6

5-chloro-pentanoic acid phenylamide

881386-01-2

3,3-dichloro-1-(4-nitrophenyl)piperidine-2-one

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: potassium hydroxide / dichloromethane; N,N-dimethyl-formamide / 1 h / 0 - 20 °C / Inert atmosphere
2: nitric acid; sulfuric acid / 0 - 5 °C
3: phosphorus pentachloride / toluene / 1 h / 25 - 80 °C
View Scheme
881386-01-2

3,3-dichloro-1-(4-nitrophenyl)piperidine-2-one

C11H12Cl2N2O

Conditions
ConditionsYield
With tin(II) chloride dihdyrate In N,N-dimethyl-formamide at 60 - 65℃; for 0.5h; Solvent; Temperature; Reagent/catalyst;90.89%
110-91-8

morpholine

881386-01-2

3,3-dichloro-1-(4-nitrophenyl)piperidine-2-one

503615-03-0

3-(morpholin-4-yl)-1-(4-nitrophenyl)-5,6-dihydropyridin-2(1H)-one

Conditions
ConditionsYield
at 120℃; for 2h; Inert atmosphere;90.4%
at 130℃; for 1.5h;87.6%
at 130℃; for 5h;64.5%
at 130℃; for 1.5h;
In N,N-dimethyl-formamide for 1h; Reflux;85.73 g
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