2234-97-1Relevant articles and documents
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Jensen
, p. 225,250 (1936)
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Production method of alkyl phosphine (by machine translation)
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Paragraph 0044-0059, (2020/12/10)
The method comprises the following steps: mixing phosphine and propylene in a solvent, then adding the photocatalyst, reacting the phosphine with propylene in 20 - 50W light irradiation, and having short reaction time, relatively simple reaction time, relatively simple post-treatment, relatively simple post-treatment, and higher yield and purity of the product compared with the prior art, and the reaction time is shorter. 1 - 12h 0 °C - 50 °C. The method comprises the following steps of: carrying out free radical reaction at a temperature and a normal pressure. (by machine translation)
Method for manufacturing acryloxypropysilane
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, (2008/06/13)
A method to manufacture acryloxypropylsilane to a high degree of purity is achieved by hydrosilation of (A) allyl acrylate or allyl methacrylate by (B) a hydrosilane compound, using (C) a platinum-containing compound as the catalyst and (D) an organic phosphorus compound as the promoter. The acryloxypropylsilane product is expressed by General Formula I where R1 represents a hydrogen or methyl group, R2 represents a hydrolyzable group, R3 represents an aryl, alkenyl or aryl group of carbon number 1-12, and n is 0, 1, 2, or 3.
