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5894-65-5 Usage

Synthesis Reference(s)

Synthetic Communications, 3, p. 185, 1973 DOI: 10.1080/00397917308062033

Check Digit Verification of cas no

The CAS Registry Mumber 5894-65-5 includes 7 digits separated into 3 groups by hyphens. The first part of the number,starting from the left, has 4 digits, 5,8,9 and 4 respectively; the second part has 2 digits, 6 and 5 respectively.
Calculate Digit Verification of CAS Registry Number 5894-65:
(6*5)+(5*8)+(4*9)+(3*4)+(2*6)+(1*5)=135
135 % 10 = 5
So 5894-65-5 is a valid CAS Registry Number.
InChI:InChI=1/C11H15NO/c1-11(2,3)12-10(13)9-7-5-4-6-8-9/h4-8H,1-3H3,(H,12,13)

5894-65-5 Well-known Company Product Price

  • Brand
  • (Code)Product description
  • CAS number
  • Packaging
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  • Detail
  • Alfa Aesar

  • (L08509)  N-tert-Butylbenzamide, 98+%   

  • 5894-65-5

  • 5g

  • 359.0CNY

  • Detail
  • Alfa Aesar

  • (L08509)  N-tert-Butylbenzamide, 98+%   

  • 5894-65-5

  • 25g

  • 1281.0CNY

  • Detail
  • Alfa Aesar

  • (L08509)  N-tert-Butylbenzamide, 98+%   

  • 5894-65-5

  • 5g

  • 359.0CNY

  • Detail
  • Alfa Aesar

  • (L08509)  N-tert-Butylbenzamide, 98+%   

  • 5894-65-5

  • 25g

  • 1281.0CNY

  • Detail
  • Alfa Aesar

  • (L08509)  N-tert-Butylbenzamide, 98+%   

  • 5894-65-5

  • 5g

  • 359.0CNY

  • Detail
  • Alfa Aesar

  • (L08509)  N-tert-Butylbenzamide, 98+%   

  • 5894-65-5

  • 25g

  • 1281.0CNY

  • Detail
  • Alfa Aesar

  • (L08509)  N-tert-Butylbenzamide, 98+%   

  • 5894-65-5

  • 5g

  • 359.0CNY

  • Detail
  • Alfa Aesar

  • (L08509)  N-tert-Butylbenzamide, 98+%   

  • 5894-65-5

  • 25g

  • 1281.0CNY

  • Detail

5894-65-5SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 13, 2017

Revision Date: Aug 13, 2017

1.Identification

1.1 GHS Product identifier

Product name N-TERT-BUTYLBENZAMIDE

1.2 Other means of identification

Product number -
Other names Benzamide,N-(1,1-dimethylethyl)

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only.
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:5894-65-5 SDS

5894-65-5Relevant articles and documents

FTIR investigation of solvent effects of N-methyl and N-tert-butyl benzamide

Jovi,Nikoli,Petrovi,Kordi,Crossed D Signakovi-Sekuli,Stojanovi

, p. 1616 - 1622 (2014)

Infrared spectroscopy studies of N-methyl benzamide and N-tert-butyl benzamide in 12 organic solvents were undretaken to investigate solvent-solute interactions. The wavenumbers of carbonyl stretching vibration ν(C=O) in different solvents were correlated

Reactions of (E)-2-tert-Butyl-3-phenyloxaziridine with Lithium Amide

Newcomb, Martin,Reeder, Robert A.

, p. 1489 - 1493 (1980)

The reactions of (E)-2-tert-butyl-3-phenyloxaziridine (1a) with lithium amide bases in tetrahydrofuran have been studied.In competing rections, 1a is reduced to N-tert-butylbenzaldimine (2) and isomerized to N-tert-butylbenzamide (3).The former reaction proceeds through an intermediate which accumulates and slowly decomposes to 2; the reaction apparently occurs via an initial electron transfer from the base to the oxaziridine.The latter reaction occurs by simultaneous deprotonation and ring opening of the oxaziridine to give the anion of 3.

AMINE-BORANES AS BIFUNCTIONAL REAGENTS FOR DIRECT AMIDATION OF CARBOXYLIC ACIDS

-

Paragraph 0008-0009; 0063-0064, (2022/03/04)

The present invention generally relates to a process for selective and direct activation and subsequent amidation of aliphatic and aromatic carboxylic acids to afford an amide R3CONR1R2. That the process is capable of delivering gaseous or low-boiling point amines provides a major advantage over existing methodologies, which involves an intermediate of triacyloxyborane-amine complex [(R3CO2)3—B—NHR1R2]. This procedure readily produces primary, secondary, and tertiary amides, and is compatible with the chirality of the acid and amine involved. The preparation of known pharmaceutical molecules and intermediates has also been demonstrated.

N,O-Benzyl Protection of Structurally Varied Amines and Phenols Using Wells-Dawson Heteropolyacid Catalyst

Boughaba, Sara,Aouf, Zineb,Zerrouki, Rachida,Aouf, Nour Eddine

, p. 301 - 310 (2021/05/24)

-

Insight into Regioselective Control in Aerobic Oxidative C-H/C-H Coupling for C3-Arylation of Benzothiophenes: Toward Structurally Nontraditional OLED Materials

Bin, Zhengyang,Liao, Xingrong,Liu, Jiahui,Shen, Boming,Shi, Yang,Yan, Lipeng,Yang, Feng,Yang, Ge,Yang, Yudong,You, Jingsong,Yu, Peiyuan

supporting information, (2021/12/14)

The installation of (benzo)thiophene-containing biaryls via coupling reactions has become a staple in designing photoelectric materials. Undeniably, C-H/C-H cross-coupling reactions between two (hetero)aromatics would be a shortcut toward these structural fragments. While more reliable cross-coupling technologies are well-established to provide C2-arylated (benzo)thiophenes, efficient methods that arylate the C3-position remain underdeveloped. Herein we provide insight into the factors that determine regioselectivity switching for these cross-coupling reactions. X-ray crystallographic analysis gives solid evidence for the key roles of triflate in regioselective dearomatization and acetate in base-assisted anti-β-deprotonated rearomatization. The first isolation and X-ray characterization of a medium-sized dearomatized cyclometalated adduct involving both substrates provide extra insight into aerobic oxidative Ar-H/Ar-H cross-coupling reactions. The mechanistic breakthrough incubates the first example, enabling C-H/C-H-type C3-arylation of benzothiophenes. Finally, this chemistry is used to design blue-emitting thermally activated delayed fluorescence (TADF) materials with a helicene conformation that exhibit a high maximum external quantum efficiency of 25.4% in OLED.

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