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611-33-6

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611-33-6 Usage

Chemical Properties

CLEAR YELLOW TO BROWN LIQUID

Synthesis Reference(s)

The Journal of Organic Chemistry, 52, p. 1673, 1987 DOI: 10.1021/jo00385a006

Purification Methods

Purify it by crystallisation of its ZnCl2 complex (m 228o) from aqueous EtOH. [Beilstein 20 III/IV 3381, 20/7 V 315.]

Check Digit Verification of cas no

The CAS Registry Mumber 611-33-6 includes 6 digits separated into 3 groups by hyphens. The first part of the number,starting from the left, has 3 digits, 6,1 and 1 respectively; the second part has 2 digits, 3 and 3 respectively.
Calculate Digit Verification of CAS Registry Number 611-33:
(5*6)+(4*1)+(3*1)+(2*3)+(1*3)=46
46 % 10 = 6
So 611-33-6 is a valid CAS Registry Number.
InChI:InChI=1/C9H6ClN/c10-8-5-1-3-7-4-2-6-11-9(7)8/h1-6H

611-33-6SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 19, 2017

Revision Date: Aug 19, 2017

1.Identification

1.1 GHS Product identifier

Product name 8-chloroquinoline

1.2 Other means of identification

Product number -
Other names Quinoline,8-chloro

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only.
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:611-33-6 SDS

611-33-6Relevant articles and documents

1-(1-Alkylsulfonic)-3-methylimidazolium chloride Br?nsted acidic ionic liquid catalyzed Skraup synthesis of quinolines under microwave heating

Amarasekara, Ananda S.,Hasan, Muhammad A.

, p. 3319 - 3321 (2014)

1-(1-Alkylsulfonic)-3-methylimidazolium chloride Br?nsted acidic ionic liquids are shown as excellent catalysts and reaction mediums for Skraup synthesis of quinolines under microwave conditions without the use of nitrobenzene as an oxidant and metal catalysts.

High efficiency microwave-assisted synthesis of quinoline from acrolein diethyl acetal and aniline utilizing Ni/Beta catalyst

Li, An,Yang, Zan,Yang, Tao,Luo, Cai-Wu,Chao, Zi-Sheng,Zhou, Cong-Shan

, p. 21 - 25 (2018/07/06)

A facile and solvent-free microwave-assisted approach to quinoline was developed by utilizing both acrolein diethyl acetal and aniline as reagents, firstly employing Ni/Beta zeolite as mild, ecofriendly and low-cost solid catalyst. As high as 83% yield of quinoline was quickly achieved at a short microwave time. The results indicated that the effect of Ni on Beta zeolite not only significantly promoted conversion of acrolein diethyl acetal to effective intermediate but also dramatically accelerated dehydrogenation rate of tetrahydroquinoline/dihydroquinoline to quinoline.

Synthesis of quinolines by iron-catalyzed reaction of anilines with propane-1,3-diol

Khusnutdinov,Bayguzina,Aminov

, p. 2725 - 2727 (2016/02/18)

Quinoline and its derivatives were synthesized by cyclocondensation of anilines with propane-1,3-diol in 57-96% yield in the presence of iron-containing catalysts in carbon tetrachloride.

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