69045-78-9

Basic information

• Product Name: 2-Chloro-5-trichloromethylpyridine
• Synonyms: IFLAB-BB F0797-0001;2-CHLORO-5-TRICHLOROMETHYL PYRIDINE;AKOS BBS-00000412;69045-78-9;2-Chloro-5-trichloromethylpyridine###NA
• CAS NO: 69045-78-9
• Molecular Formula: C₆H₃Cl₄N
• Molecular Weight: 230.90672
• EINECS: 1308068-626-2
• Product Categories: Halides;Pyridines;Pyridine;API Intermediate;Heterocycle-Pyridine series;Imidazoles
• Mol File: 69045-78-9.mol
• Article Data: 21

Chemical Properties

• Melting Point: -18.14 °C
• Boiling Point: 281.8°C at 760 mmHg
• Flash Point: 151.2 °C
• Appearance: /
• Density: 1.582 g/cm³
• Vapor Pressure: 0.00596mmHg at 25°C
• Refractive Index: 1.575
• Storage Temp.: under inert gas (nitrogen or Argon) at 2-8°C
• PKA: -2.26±0.10(Predicted)
• CAS DataBase Reference: 2-Chloro-5-trichloromethylpyridine(CAS DataBase Reference)
• NIST Chemistry Reference: 2-Chloro-5-trichloromethylpyridine(69045-78-9)
• EPA Substance Registry System: 2-Chloro-5-trichloromethylpyridine(69045-78-9)

Safety Data

• Hazard Codes: Xi,T
• Statements: 36/37/38-25
• Safety Statements: 26-37/39-45
• RIDADR: UN2811
• Hazardous Substances Data: 69045-78-9(Hazardous Substances Data)

Usage

General Description

2-Chloro-5-trichloromethylpyridine is a chemical compound with the molecular formula C6H3Cl4N. It is primarily used as a pesticide and herbicide due to its ability to control a wide range of pests and weeds. The compound is highly toxic and poses serious health risks to humans and animals if not handled and used with caution. Exposure to 2-Chloro-5-trichloromethylpyridine can result in skin and eye irritation, respiratory issues, and even more severe health problems if ingested or inhaled. Proper safety measures and protective equipment should be used when handling this chemical, and its use should be strictly regulated to minimize its potential harm to the environment and living organisms.

InChI:InChI=1/C6H3Cl4N/c7-5-2-1-4(3-11-5)6(8,9)10/h1-3H

Upstream product

• 18368-64-4 2-chloro-5-methylpyridine 
• 108-99-6 3-Methylpyridine 
• 5006-66-6 6-hydroxy-3-pyridinecarboxylic acid 
• 59-67-6 nicotinic acid 
• 3099-50-1 3-trichloromethyl-pyridine 
• 70258-18-3 2-chloro-5-(chloromethyl)pyridine 
• 52334-81-3 2-chloro-5-trifluoromethylpyridine 
• 3510-66-5 2-Bromo-5-methylpyridine 

Downstream Products

• 120739-62-0 1-(6-chloropyridin-3-yl)-N-methylmethanamine 
• 101990-44-7 N'-((6-chloropyridin-3-yl)methyl)ethane-1,2-diamine 
• 5326-23-8 6-Chloro-3-pyridinecarboxylic acid 
• 58584-80-8 2,3,6-trichloro-5-(trichloromethyl)pyridine 
• 69045-82-5 2-fluoro-5-(trifluoromethyl)pyridine 
• 70258-18-3 2-chloro-5-(chloromethyl)pyridine 
• 69045-84-7 2,3-dichloro-5-trifluoromethylpyridine 
• 69045-83-6 2,3-dichloro-5-(trichloromethyl)pyridine 
• 71422-67-8 chlorfluazuron 
• 73265-15-3 3,5-dichloro-4-[(3-chloro-5-(trifluoromethyl)pyridin-2-yl)oxy]aniline 
• 217096-52-1 NC₅H₃-6-Cl-3-CCo₃(CO)9 
• 217096-53-2 NC₅H₄-3-CCo₃(CO)9 
• 52334-81-3 2-chloro-5-trifluoromethylpyridine 
• 71701-84-3 2-chloro-5(chlorodifluoromethyl)pyridine 

Relevant articles and documents

Synthesis, characterization and crystal structure of 2,3,6-trichloro-5- (trichloromethyl)pyridine

2,3,6-Trichloro-5-(trichloromethyl)pyridine (TCTCMP) was synthesized from 2-chloro-5-chloromethyl pyridine (CCMP) through two-steps chloridization using chlorine as chlorizating agent. Initially, 2-chloro-5-chloromethyl pyridine was chloridized for 8 h at reflux conditions in the presence of ultraviolet and transformed into 2-chloro-5-(trichloromethyl)pyridine (CTCMP), then CTCMP was chloridized for 6 h at 175 °C with WCl6 as catalyst. The product was characterized by FT-IR, NMR and elemental analysis. The crystal structure of TCTCMP was investigated using X-ray diffraction and SHELXTL97 software and the result indicated that TCTCMP crystallized in the orthorhombic system, space group Pbcm with a = 8.3100(17), b = 17.018 (3), c = 7.3160(15) A, V = 1034.6 (4) A3; Z 4.

2-chloro-5-trichloromethyl pyridine rectification purification method and device

The invention discloses a 2-chloro-5-trichloromethyl pyridine rectification purification method and device. Rectification purification of 2-chloro-5-trichloromethyl pyridine is implemented by using adevice for rectification purification of 2-chloro-5-trichloromethyl pyridine. By adopting the device for rectification purification of the 2-chloro-5-trichloromethyl pyridine, purification of a crudeproduct of 2-chloro-5-trichloromethyl pyridine can be efficiently implemented, the device is simple in structure and low in cost, and together with a purification method for the crude product of the 2-chloro-5-trichloromethyl pyridine, the purification rate of the crude product of the 2-chloro-5-trichloromethyl pyridine can be greatly increased.

A 2 - chloro -5 - nitrapyrin preparation method

The invention discloses a 2 - chloro - 5 - trichloromethyl pyridine method, comprises the following steps: (1) the 3 - methyl pyridine is mixed with a solvent, the vaporization of the drops in the vaporization vessel, then in order to inert gas as a carrier gas, to form raw material steam; (2) dry Cl respectively2 The raw material and the steam is sent to the quartz tube catalyst [...] generating vapor phase chlorination reaction, reaction material after the condensation, rectification to obtain 2 - chloro - 5 - trichloromethyl pyridine. The invention relates to a 2 - chloro - 5 - trichloromethyl pyridine method, with raw materials are easy, low cost, easy to operate, simple process and the like.