Synthesis and molecular structure of 2-bromo-N-(4-(7-(diethylamino)-coumarin-3-yl)phenyl)propanamide: New coumarin-based fluorescent ATRP initiator

Add time:07/13/2019    Source:sciencedirect.com

The 2-bromo-N-(4-(7-(diethylamino)-coumarin-3-yl)phenyl)propanamide was synthesized and analyzed by NMR and FT-IR spectroscopies, high resolution mass-spectrometry and single crystal X-ray diffraction. The crystal structure belongs to the monoclinic system, P21/c space group with a = 14.9120(7) Å, b = 11.3177(5) Å, c = 12.0106(5) Å, α = 90°, β = 94.758(2)°, γ = 90° and V = 2020.04(16) Å3. Furthermore, it was shown to be an efficient fluorescent ATRP initiator in polymerizations of acrylates.

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