Effect of heat treatment conditions on magnesium borate (cas 12007-62-4) fibers prepared via electrospinning

Add time:07/24/2019    Source:sciencedirect.com

The influence of different heating rates as well as different atmospheres on magnesium borate (cas 12007-62-4) fibers produced by electrospinning was investigated in this work. The green fibers were prepared from sol–gel precursors, using polyvinyl-pyrrolidone (PVP) as processing aid. Crystalline fibers with the typical necklace structure and average diameter in the range 300–500 nm were produced when heating up to 900 °C in air. The main phase detected by XRD analysis was in this case Mg2B2O5. On the other hand, the fibers slowly heated in reducing atmosphere to 800 °C exhibited similar dimension but a different morphology. The crystalline grains were presumably smaller, hence the necklace effect was absent. This sample also revealed a much higher specific surface area in comparison to the samples calcined in air. Mg3B2O6 was here the main crystalline phase, while a part of boron was lost during the thermal treatment.

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