Optical properties of the mechanochemically synthesized Cu2FeSnS4 (stannite (cas 12019-29-3)) nanocrystals: Raman study

Add time:07/27/2019    Source:sciencedirect.com

The analysis of the vibrational properties of mechanochemically synthesized stannite Cu2FeSnS4 nanocrystals has been performed. X-ray diffraction (XRD) and Raman spectroscopy are techniques used to characterize the crystal structure and compositional purity of stannite Cu2FeSnS4 nanoparticles. The detailed analysis of the experimental spectra has allowed us to determine the frequency and symmetry assignment of the main and weaker peaks. The milling time influence on synthesis stannite Cu2FeSnS4 from elemental precursors Cu, Fe, Sn and S is observed. Among the peaks that are characteristic for the stannite Cu2FeSnS4, we registered the modes of binary phases of FeS and SnS. The total disappearance of the binary phases of FeS and SnS is observed when the milling time is longer than 90 min.

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