Structural features and magnetic behavior of nanocrystalline powders of Terbium oxide (cas 12035-91-5) prepared by the thermal decomposition of terbium acetate in air

Add time:07/29/2019    Source:sciencedirect.com

Nanostructured powders of Terbium oxide (cas 12035-91-5)s were prepared by the thermal decomposition of terbium acetate at different temperatures. The powders were investigated by means of XRD, HRTEM, magnetic measurements, and IR spectroscopy. It has been found that the most likely composition of the oxides is Tb4O7, and the powders containing more than one crystalline phase. At low temperatures the prepared oxides exhibit antiferromagnetic ordering with the Weiss constants ranging from −14 to −22 K. At 2 K the effective value of total angular momentum per one Tb ion in the paramagnetic state J = 2.5 ± 0.1. The effects of the calcination temperature on the crystal structure, microstructure and magnetic behaviors of the samples are discussed in terms of that surface impurities presented in the nanocrystalline powders of Tb oxides influence the cation Tb4+/Tb3+ ratio in their crystal lattice.

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