Photolysis of chloride precursors as a method to prepare and characterize the triplet state of fluorenyl-substituted m-xylylene diradicals
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Add time:08/05/2019 Source:sciencedirect.com
Fluorenyl substituted m-xylylene triplet diradicals are conveniently generated from the corresponding dichloride precursors upon photolysis at <100 K in 2-MeTHF glass. Under similar conditions tert-butyl substituted Schlenk type m-xylylene could not be generated from the dichloride precursor 6. Compound 6, however could be dehalogenated with zinc dust in both toluene and 2-MeTHF to produce the triplet diradical.
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