A multigram, stereoselective synthesis of d

Add time:08/09/2019    Source:sciencedirect.com

The preparation of 13C-labeled ribonucleosides starting from d-[13C6]glucose in 45% overall yield is described. The key of this short synthetic way is the dehomologation of di-O-isopropylidene hexofuranose 2 with periodic acid and NaBH4 that afforded stereoselectively the labeled ribofuranose derivative 3 in high yield.

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