Synthesis,characterization of 1-butyl-4-methylpyridinium lauryl sulfate and its inclusion phenomenon with β-cyclodextrin for enhanced applications
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Add time:08/19/2019 Source:sciencedirect.com
1-Butyl-4-methylpyridinium lauryl sulfate was synthesized and a number of spectroscopic techniques were used for the characterization. The surface active property was explored in different ways. The Host Guest inclusion complex formation with the synthesized compound inside the β-Cyclodextrin has been studied qualitatively as well as quantitatively with physicochemical, spectroscopic and advanced microscopic techniques. The Job plot from the UV–vis spectroscopy indicates the formation of both 1:1 and 2:1 inclusion. The inclusion complex has given the determining morphology with further evidence of 2:1 inclusion in HRTEM supported by DLS. Lastly, the 2D-NOESY has provided a conclusive mechanism for the inclusion phenomenon.
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