Practical and concise synthesis of 2-oxo-3,4,5,6-tetraethoxyazepane from D-Glucono-1,5-lactone (cas 1335-57-5)
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Add time:09/06/2019 Source:sciencedirect.com
2-Oxo-3R,4S,5S,6S-tetraethoxyazepane was conveniently synthesized from d-glucono-1, 5-lactone with a yield of 10% overall. The key step of synthetic route-reductive 1,6-cyclization was completed efficiently by using Ph3P to give the expected lactam.
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