Crystal structure and FT-IR study of cesium 4-methylbenzenesulfonate

Add time:09/07/2019    Source:sciencedirect.com

The crystal structure of the title compound has been determined by X-ray diffraction. The crystal is monoclinic, space group P21/C with a=13.483(3)A, b=7.285(1)A, c=10.352(2)A, β=110.43(3)°, and Z=4, V=952.8(3)A3, Dc=2.120 g cm−3, λ(MoKα)=0.71073A, μ=4.033 mm−1, F(000)=576, final weighted R=0.0391 for 1863 unique reflections. The cesium atom is coordinated to six oxygen atoms from five sulfonate groups to form a distorted octahedron. There is no water molecule and no H-bond network in the complex. FT-IR spectra was also used to characterize the complex. A preliminary infrared assignment was performed.

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