Mild propargylic oxidation using a diacetoxyiodobenzene/tert-butyl hydroperoxide protocol
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Add time:09/24/2019 Source:sciencedirect.com
A mild propargylic oxidation of alkynes is reported using a diacetoxyiodobenzene/tert-butyl hydroperoxide (DIB/TBHP) protocol. The reactions proceed smoothly at 0 °C and a number of α,β-unsaturated alkynoic ketones are obtained.
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