First total synthesis of 6-tuliposide B
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Add time:09/26/2019 Source:infona.pl
Labile (+)-6-tuliposide B, an antimicrobial compound produced by tulip, was synthesized in nine steps from d-glucose via the Baylis–Hillman reaction of 2-(tert-butyldimethylsilyloxy)-acetaldehyde with 6-O-acryloyl-1-O-(2-trimethylsilylethyl)-β-d-glucopyranoside, followed by a mild deprotection procedure using TFA in CH 2 Cl 2 .
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