The synthesis of iron (III) ethoxide revisited: Characterization of the metathesis products of iron (III) halides and Sodium ethoxide (cas 141-52-6)

Add time:10/01/2019    Source:infona.pl

Interaction of FeX 3 , X=Cl, Br with 3 equiv. of NaOEt in toluene/ethanol media provides mixtures of iron (III) oxoethoxide, Fe 5 O(OEt) 13 , and its halide alkoxide analogs. The latter have been identified by mass-spectrometric study as Fe 5 O(OEt) 12 X and Fe 5 O(OEt) 11 X 2 . Application of FeBr 3 as a starting material leads to much more pure samples of Fe 5 O(OEt) 13 isolated with higher yields.

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