Reductive silylation of gem-difluorinated Phosphonium (cas 16749-13-6) salts
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Add time:07/21/2019 Source:sciencedirect.com
gem-Difluorinated Phosphonium (cas 16749-13-6) salts, generated from aldehydes and difluorinated phosphobetaine reagent, were converted into corresponding silicon reagents. The reductive silylation of carbon-phosphorus bond is carried out using a combination of magnesium and chlorotrimethylsilane in dimethylformamide. For a model difluoroined phosphonium salt, X-ray structure and reduction potential are provided.
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