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Cas Database |
| Name |
2,5-Furandimethanol |
EINECS | 217-544-1 |
| CAS No. | 1883-75-6 | Density | 1.283 g/cm3 |
| PSA | 53.60000 | LogP | 0.26420 |
| Solubility | N/A | Melting Point |
74-77 °C |
| Formula | C6H8O3 | Boiling Point | 275.4 °C at 760 mmHg |
| Molecular Weight | 128.128 | Flash Point | 120.3 °C |
| Transport Information | N/A | Appearance | Off-white to pale yellow solid |
| Safety | 24/25 | Risk Codes | N/A |
| Molecular Structure |
|
Hazard Symbols | N/A |
| Synonyms |
2,5-Bis(hydroxymethyl)furan;2,5-Di(hydroxymethyl)furan;5-(Hydroxymethyl)furfuryl alcohol;FaRez 6305;NSC40737;NSC 524614; |
Article Data | 153 |
2,5-Furandimethanol Synthetic route
| Conditions | Yield |
|---|---|
| With hydrogen; 3mol% Pt/C In ethanol at 20℃; under 3750.38 Torr; for 48h; Product distribution / selectivity; | 100% |
| With methanol; magnesium oxide at 160℃; under 750.075 Torr; for 3h; Meerwein-Ponndorf-Verley Reduction; Autoclave; Inert atmosphere; chemoselective reaction; | 100% |
| With sodium tetrahydroborate In water | 100% |
- 67-47-0
5-hydroxymethyl-2-furfuraldehyde
A
- 1883-75-6
2,5-bis-(hydroxymethyl)furan
B
- 6338-41-6
5-hydroxymethyl-furan-2-carboxylic acid
| Conditions | Yield |
|---|---|
| Stage #1: 5-hydroxymethyl-2-furfuraldehyde With potassium hydroxide Cannizzaro Reaction; Milling; Inert atmosphere; Sealed tube; Green chemistry; Stage #2: With hydrogenchloride In water for 0.0833333h; Reagent/catalyst; Time; Green chemistry; | A 99% B 99% |
| With sodium dithionite; sodium hydroxide In water Cannizzaro Reaction; | A 96% B 94% |
| With sodium hydroxide In water; isopropyl alcohol at 20℃; for 16h; Solvent; Cannizzaro Reaction; Microwave irradiation; | A 30% B 31 %Chromat. |
- 69924-30-7
5-hydroxymethyl-tetrahydrofuran-2-carbaldehyde
A
- 104-80-3, 1122-89-0, 2144-40-3, 81370-88-9, 81370-89-0
tetrahydrofuran-2,5-dimethanol
B
- 1883-75-6
2,5-bis-(hydroxymethyl)furan
| Conditions | Yield |
|---|---|
| With hydrogen In 1,4-dioxane at 60℃; under 45004.5 Torr; for 6h; Catalytic behavior; Reagent/catalyst; Overall yield = 100 %; | A 96.2% B 3.6% |
| Conditions | Yield |
|---|---|
| With sodium tetrahydroborate In methanol Cooling; | 94% |
| Stage #1: 2,5-diformylfurane With phenylsilane; caesium carbonate In 2-methyltetrahydrofuran at 25℃; for 1h; Green chemistry; Stage #2: With ethanol In 2-methyltetrahydrofuran at 80℃; for 2h; Green chemistry; chemoselective reaction; | 87% |
| With trans-Ru(mer-2-(4-phenyl-1H-1,2,3-triazol-1-yl)-N-(pyridin-2-ylmethyl)ethan-1-amine)(PPh3)Cl2; potassium tert-butylate; hydrogen In tetrahydrofuran at 80℃; under 7500.75 Torr; Autoclave; Sealed tube; | 52% |
- 67-47-0
5-hydroxymethyl-2-furfuraldehyde
A
- 620-02-0
5-Methylfurfural
B
- 1883-75-6
2,5-bis-(hydroxymethyl)furan
| Conditions | Yield |
|---|---|
| With hydrogen; 20Cu/Al2O3 In methanol at 130℃; under 22502.3 Torr; for 1h; Catalytic behavior; Solvent; | A 6.62% B 93.01% |
| With water; hydrogen at 160℃; under 30003 Torr; for 4h; Autoclave; | |
| With hydrogen In ethanol at 100℃; under 37503.8 Torr; for 6h; Autoclave; |
- 10551-58-3
5-acetoxymethyl-2-furaldehyde
- 1883-75-6
2,5-bis-(hydroxymethyl)furan
| Conditions | Yield |
|---|---|
| With sodium tetrahydroborate In methanol at 20℃; for 0.5h; | 92% |
| Stage #1: 5-acetoxymethyl-2-furaldehyde With sodium tetrahydroborate In ethanol at 0 - 20℃; for 48h; Stage #2: With hydrogenchloride In ethanol at 0℃; pH=4; | 91% |
- 67-47-0
5-hydroxymethyl-2-furfuraldehyde
- 67-63-0
isopropyl alcohol
A
- 1883-75-6
2,5-bis-(hydroxymethyl)furan
| Conditions | Yield |
|---|---|
| With ZnO-ZrO2/USY(Si/Al-7) at 180℃; for 2.5h; Reagent/catalyst; Autoclave; | A 6.6% B 91.4% |
| With ZrO2/Beta1401 at 150℃; for 2.5h; Reagent/catalyst; Autoclave; | A 22.8% B 16.4% |
- 67-47-0
5-hydroxymethyl-2-furfuraldehyde
A
- 1883-75-6
2,5-bis-(hydroxymethyl)furan
B
- 1356930-86-3
5-hydroxymethylfuran-2-carboxylic acid sodium
| Conditions | Yield |
|---|---|
| With sodium hydroxide In water at 0 - 20℃; for 19h; Reagent/catalyst; Solvent; Temperature; Concentration; Cannizzaro Reaction; Green chemistry; | A 90% B 85% |
- 1883-75-6
2,5-bis-(hydroxymethyl)furan
| Conditions | Yield |
|---|---|
| With NiRe0.5/TiO2; hydrogen; sodium carbonate In water at 40℃; under 37503.8 Torr; for 4h; pH=10.4; Reagent/catalyst; pH-value; Autoclave; Glovebox; | 89% |
| Multi-step reaction with 2 steps 1: sodium carbonate; Ni/TiO2; hydrogen / water / 4 h / 40 °C / 37503.8 Torr / pH 10.4 / Autoclave; Glovebox 2: Ni/TiO2; hydrogen / water / 4 h / 40 °C / 37503.8 Torr / Autoclave; Glovebox View Scheme | |
| Multi-step reaction with 2 steps 1: NiRe0.5/TiO2; hydrogen / water / 4 h / 40 °C / 37503.8 Torr / pH 7 / Autoclave; Glovebox 2: Ni/TiO2; hydrogen / water / 4 h / 40 °C / 37503.8 Torr / Autoclave; Glovebox View Scheme |
- 67-47-0
5-hydroxymethyl-2-furfuraldehyde
- 64-17-5
ethanol
A
- 1883-75-6
2,5-bis-(hydroxymethyl)furan
B
- 99181-63-2
2,5-furandimethanol diethyl ether
| Conditions | Yield |
|---|---|
| With BaO-ZrO2/SBA-15 at 150℃; for 4h; Reagent/catalyst; Time; Temperature; Autoclave; | A 88.6% B 5.2% |
2,5-Furandimethanol Chemical Properties
Molecule structure of 2,5-Furandimethanol (CAS NO.1883-75-6):
IUPAC Name: [5-(Hydroxymethyl)furan-2-yl]methanol
Molecular Weight: 128.12592 g/mol
Molecular Formula: C6H8O3
Density: 1.283 g/cm3
Melting Point: 74-77 °C
Boiling Point: 275.4 °C at 760 mmHg
Flash Point: 120.3 °C
Index of Refraction: 1.542
Molar Refractivity: 31.45 cm3
Molar Volume: 99.8 cm3
Polarizability: 12.46×10-24 cm3
Surface Tension: 52.1 dyne/cm
Enthalpy of Vaporization: 54.27 kJ/mol
Vapour Pressure: 0.00248 mmHg at 25 °C
XLogP3-AA: -0.7
H-Bond Donor: 2
H-Bond Acceptor: 3
Rotatable Bond Count: 2
Exact Mass: 128.047344
MonoIsotopic Mass: 128.047344
Topological Polar Surface Area: 53.6
Heavy Atom Count: 9
Complexity: 74.4
Canonical SMILES: C1=C(OC(=C1)CO)CO
InChI: InChI=1S/C6H8O3/c7-3-5-1-2-6(4-8)9-5/h1-2,7-8H,3-4H2
InChIKey: DSLRVRBSNLHVBH-UHFFFAOYSA-N
EINECS: 217-544-1
Product Categories: Detergents;Mutagenesis Research Chemicals
2,5-Furandimethanol Specification
2,5-Furandimethanol (CAS NO.1883-75-6) is also named as 2,5-Bis(hydroxymethyl)furan ; NSC 40737 ; NSC 524614 ; 2,5-Furandimethanol ; Furan-2,5-diyldimethanol . 2,5-Furandimethanol (CAS NO.1883-75-6) is off-white to pale yellow solid.
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