cas 13505-41-4, 4,4,4-TRICHLORO-3-HYDROXY-1-PHENYL-BUTAN-1-ONE | Articles data ｜lookchem

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13505-41-4

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First synthesis of 1-aryl-4,4-dichlorobut-3-en-1-ones. The electrochemical reduction of 1-aryl-4,4,4-trichlorobut-2-en-1-ones as a key step
The first method for the synthesis of 1-aryl-4,4-dichlorobut-3-en-1-ones is reported. Treatment of acetophenones with anhydrous chloral leads to 1-aryl-4,4,4-trichloro-3-hydroxybutan-1-ones in near quantitative yields. These compounds were efficiently deh
Guirado, Antonio,Martiz, Bruno,Andreu, Raquel,Bautista, Delia,Gálvez, Jesús
p. 1175 - 1182
(2007/10/03)

First synthesis of 3-aryl-5-dichloromethyl-2-pyrazolines. The electrochemical generation of 2,2-dichlorovinylacetophenones as a key step
An efficient synthetic route to the title compounds has been established. Chloralacetophenones 2 were prepared by treatment of acetophenones 1 with anhydrous chloral. Dehydration of intermediates 2 under acidic conditions yielded 2,2,2-trichloroethylidene
Guirado, Antonio,Martiz, Bruno,Andreu, Raquel
p. 8523 - 8526
(2007/10/03)

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Chemical Properties

Boiling Point: 396.2 °C at 760 mmHg
Flash Point:193.4 °C
Density: 1.437 g/cm³
Vapor Pressure: 5.46E-07mmHg at 25°C
Refractive Index: 1.575
PSA: 37.30000
LogP: 2.99050

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