- Purification of Allyl cyanide (3-Butene nitrile)
-
It should be redistd at atmospheric pressure then distilled under a vacuum to remove final traces of HCN from the residue. Note that the residue from the first distiln may be difficult to remove from the flask and should be treated with conc HNO3 then H2O and finally hot EtOH (CARE). Allyl cyanide (CAS NO. ) has an onion-like odour and is stable to heat. It forms a complex with AlCl3 (2:2) m 41 °C, and (3:2) m 120 °C.
All operations should be done in an efficient fume hood as the liquid is flammable and highly toxic.
Prev:No record
Next:No record - 【Back】【Close 】【Print】【Add to favorite 】
- Related information
- One Synthetic Approach of Trimethylene cyanide
- Synthetic Approach of p-Nitrobenzyl cyanide
- Preparation of Allyl cyanide
- Production Method of Allyl lactate
- One Synthetic Approach of Benzoyl cyanide
- Synthetic Approach of Methanesulfonyl cyanide
- Production Method of Diaminomaleonitrile (hydrogen cyanide tetramer)
- Preparation of Allyl alcohol
- Synthetic Method of Carbonyl cyanide
- Synthetic Method of Cyclopropyl cyanide
-
Health and Chemical more >
-
Hot Products
- 118-69-4 Benzene,1,3-dichloro-2-methyl-
- 2044-64-6 N,N-Dimethylacetoacetamide
- 30635-27-9 argipressin, Phe(2)-
- 108-65-6 1-Methoxy-2-propyl acetate
- 1885-14-9 Phenyl chloroformate
- 886762-81-8 2,3,6-Trifluorophenacyl bromide
- 25766-16-9 Silane, dichlorodimethyl-, polymer with trichloromethylsilane and trichlorophenylsilane
- 51-66-1 Acetamide,N-(4-methoxyphenyl)-
- 1302-09-6 SILVER SELENIDE
- 19184-10-2 (Z)-1-Fluoro-1-propene
- 1405-86-3 Glycyrrhizic acid
- 503-17-3 2-Butyne