GENERAL SYNTHESIS OF 2,5-DIHYDROTHIOPHENES (3-THIOLENES) FROM DIKETO SULFIDES

DOI: 10.1016/S0040-4039(00)98357-6

Source and publish data:

Tetrahedron Letters p. 1981 - 1982 (1985)

Update date:2022-09-26

Topics:

Authors:

Nakayama, Juzo

Machida, Haruki

Hoshino, Masamatsu

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Article abstract of DOI:10.1016/S0040-4039(00)98357-6

The intramolecular reductive coupling reaction of easily accesible diketo sulfides by a low-valent titanium reagent (prepared from titanium(IV) chloride and zinc powder) provides an efficient general synthesis of 2,5-dihydrothiophenes.

Full text of DOI:10.1016/S0040-4039(00)98357-6

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