O-TBS-N-tosylhydroxylamine: A reagent for facile conversion of alcohols to oximes

DOI: 10.1021/ol800677p

Source and publish data:

Organic Letters p. 2259 - 2261 (2008)

Update date:2022-08-04

Topics:

Authors:

Kitahara, Katsushi

Toma, Tatsuya

Shimokawa, Jun

Fukuyama, Tohru

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Article abstract of DOI:10.1021/ol800677p

(Chemical Equation Presented) A variety of oximes were synthesized from the corresponding alcohols, alkyl halides, or alkyl sulfonates without using external oxidants. With this simple two-step procedure involving substitution with readily available TsNHOTBS and subsequent treatment with CsF, a range of oximes were prepared including the ones hardly preparable with conventional procedures.

Full text of DOI:10.1021/ol800677p

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