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Å, b = 8.3209 (3) Å, c = 17.0354 (7) Å, a = 90°, b = 96.144
(2)°, g = 90°, V = 1024.57 (7) Å3, space group P2(1)/n,
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wR2 = 0.1119. The crystallographic data for 19 have been
deposited with the Cambridge Crystallographic Data Centre.
Copies of this information may be obtained free of charge
from the Director, CCDC, 12 Union Road, Cambridge, CB2
1EZ, UK [Fax: +44 (1223)336033, e-mail:
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Synthesis 2008, No. 5, 807–819 © Thieme Stuttgart · New York