New procedure for the preparation of 2-(trimethylsilyl)ethyl 2-acetamido-2-deoxy-3,4,6-tri-O-acetyl-β-D-glucopyranoside and other alkyl β-glycosides

DOI: 10.1016/0040-4039(95)02233-3

Source and publish data:

Tetrahedron Letters p. 609 - 610 (1996)

Update date:2022-07-29

Topics: Characterization Acetylation Purification Workup Final Deprotection Deacetylation Protection of glucose

Authors:

Sowell, C. Gregory

Livesay, Mark T.

Johnson, David A.

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Article abstract of DOI:10.1016/0040-4039(95)02233-3

The title compound and other alkyl β-glycosides 1a-g can be prepared in one step from commercially available 2-acetamido-2-deoxy-1,3,4,6-tetra-O-acetyl-β-D-glucopyranose (3) and simple alcohols using camphorsulfonic acid as a promoter together with azeotr

Full text of DOI:10.1016/0040-4039(95)02233-3

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