
Journal of Organic Chemistry p. 3926 - 3934 (2017)
Update date:2022-08-04
Topics:
Lloyd, Dina
Bylsma, Marissa
Bright, Danielle K.
Chen, Xizhao
Bennett, Clay S.
The use of a combination of 2,3-dichloro-5,6-dicyano-1,4-benzoquinone (DDQ) and β-pinene permits the removal of 2-naphthylmethyl (Nap) ether protecting groups on highly sensitive substrates. The reaction tolerates both acid and base sensitive protecting groups, and products are afforded in 68-96% yield. The utility of the method is demonstrated by the removal of the Nap protecting groups on highly sensitive 2,6-dideoxy-sugar disaccharides.
Chongqing KonAo Health Co.,Ltd
Contact:13687578375
Address:wuhan hubei china
Taizhou YOJOY Chemical Co., Ltd.
Contact:13857143241
Address:Yangfu Industrial Park, Xianju, Zhejiang, P. R. China
Yangling Ciyuan biotech Co., Ltd.
Contact:86-15802970736
Address:2-1804, International Park Mansion, No.2, South Fengdeng Road, Lianhu District
shandong zhongke taidou chemical co.,ltd
Contact:86-531-88682301
Address:Jinan shandong Province CHina
Contact:+86-535-8888888
Address:No.161 Haishi Rd.
Doi:10.1016/0008-6215(95)00324-X
(1996)Doi:10.1002/adsc.201500858
(2016)Doi:10.1039/b613561g
(2007)Doi:10.1021/jm00384a026
(1987)Doi:10.1016/j.ejmech.2008.01.014
(2008)Doi:10.1002/ejoc.200701197
(2008)