Journal of Organic Chemistry p. 1288 - 1290 (1987)
Update date:2022-08-03
Topics: Regioselectivity Yield Alcohols Deprotonation Nucleophilic addition Workup Reaction Mechanism Solvent Effects Substituent Effects Tautomerization Electrophilic center Adduct formation Spectroscopic analysis (NMR, IR, MS) Chromatography (TLC, HPLC)
Mackay, Donald
Taylor, Nicholas J.
Wigle, Ian D.
The title azo compound (1) reacts with alcohols to give 1-(alkoxycarbonyl)-2-(N-phenylcarbamoyl)-4-phenyl-1,2,4-triazolidine-3,5-diones (2), the structures originally assigned to them.The X-ray diffraction analysis of the butyl compound 2c is described, together with details of its synthesis from 1 and from the parent urazole 7.
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Doi:10.1021/jo01072a614
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