Tetrahedron Letters p. 3283 - 3286 (1988)
Update date:2022-08-03
Topics:
Hudlicky, Tomas
Radesca-Kwart, Lilian
Li, Liang-quan
Bryant, Teresa
The total synthesis of retigeranic acid 1 was achieved in 14 steps from menthene.The key features involved the vinylcyclopropanation of enone 6 with the dienolate anion of 5 to furnish vinylcyclopropane 4 and its rearrangement to pentacycle 3 in an overall <2+3> cyclopentene annulation sequence.
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