CONTRIBUTION TO THE CHEMISTRY OF SILICON-SULPHUR COMPOUNDS XLII. BIS(1-METHYLDIBENZOSILOLE)SULPHIDE: ITS SYNTHESIS, CRYSTAL STRUCTURE, AND REACTION WITH CHROMIUM HEXACARBONYL

Article abstract of DOI:10.1016/0022-328X(86)80316-3

The reaction of 1-methyldibenzosilole with elemental sulphur gave almost quantitatively bis(1-methyldibenzosilole)sulphide (I), the structure of which was determined by X-ray diffraction.The crystals are monoclinic, space group P2₁/n (No. 14) w