Synthesis of an Isotopically Labeled Dilactam-Bridged Tetrapeptide

DOI: 10.1021/jo00233a007

Source and publish data:

Journal of Organic Chemistry p. 5342 - 5349 (1987)

Update date:2022-08-04

Topics: Synthesis NMR spectroscopy Mass spectrometry HPLC Purification Tetrapeptide Solid-Phase Peptide Synthesis Isotopically labeled

Authors:

Manesis, Nick J.

Goodman, Murray

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Article abstract of DOI:10.1021/jo00233a007

To aid in assigning the amide proton resonances in the NMR spectrum of the dilactam-bridged tetrapeptide derivative Ac-L--D--NHMe, an isotopically labeled analogue was synthesized.The compound was deuteriated in the C_α positio

Full text of DOI:10.1021/jo00233a007

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