Tetrahedron Letters p. 4331 - 4334 (1996)
Update date:2022-09-26
Topics:
Shi, Xiao-Xin
Khanapure, Subhash P.
Rokach, Joshua
A novel method for the deblocking of the dithioacetals and oxathioacetals is described. Periodic acid under nonaqueous conditions has been used for the deprotection of the dithio- and oxathio-derivatives to the corresponding carbonyl compounds. This simple high-yield transformation is conveniently carried out in nonaqueous medium and works well with complex sensitive aldehydes and in the presence of other protective groups.
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