Phosphorus, Sulfur and Silicon and the Related Elements p. 871 - 878 (2012)
Update date:2022-09-26
Topics:
Bardajee, Ghasem Rezanejade
Afsari, Hamid Samareh
Sadraei, Seyediraj
Taimoory, Seyedehmaryamdokht
An efficient, versatile, and environmentally benign method for the synthesis of dithiocarbamates under solvent-free conditions is reported. The Michael addition of electron-deficient alkenes with alkyl or aryl amines and CS2 in the presence of OH-/silica in a one-pot three-component reaction protocol gave the corresponding dithiocarbamates in good to excellent yields. This method is suitable for a wide range of amines and a variety of Michael acceptors in solvent-free conditions. The results of the present work show the desired products in excellent yields. Copyright Taylor and Francis Group, LLC 2012.
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