Chemistry Letters p. 1801 - 1804 (1988)
Update date:2022-07-30
Topics:
Tanaka, Hideo
Tanaka, Motoaki
Hironaka, Yo-ichi
Nakai, Akira
Torii, Sigeru
A straightforward access to penicillinates bearing SCN and SeCN groups at the 2β-methyl group was performed by electrolysis of 4-dithioazetidinones in a two-phase system (aqueous and organic phases) in the presence of KSCN and KSeCN, respectively, while a mixture of 2β-azidomethyl derivative and its 2α-isomer (6/4) was obtained by a similar electrolysis with NaN3.
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