Synthetic Communications p. 506 - 515 (2009)
Update date:2022-08-05
Topics:
Bang, Hyun Bae
Han, Su Young
Choi, Da Hye
Yang, Deok Mo
Hwang, Jung Woon
Lee, Hyun Suck
Jun, Jong-Gab
An efficient and practical total synthesis of benzo[b]furan natural product XH-14 is demonstrated in nine steps from vanillin. Introduction of iodide substituents in the reaction including optimization of the reaction sequences is essential for the successful synthesis of XH-14. Sonogashira coupling with iodobenzene, iodine-induced cyclization, Wittig reaction, and formylation are critical in the high-yield total synthesis of XH-14. Copyright Taylor & Francis Group, LLC.
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