Journal of the Chemical Society, Dalton Transactions p. 2793 - 2802 (1987)
Update date:2022-07-29
Topics:
Alcock, Nathaniel W.
Jasztal, Michael J.
Wallbridge, Malcolm G. H.
The reaction of A phosphine ligand is transferred from the metal atom to the cage in each case, and they both show a decarborane(14)-like cage structure with the 6- and 9-positions occupied by CH and M(CO)(PPh3)2 fragments respectively, as confirmed by single-crystal X-ray diffraction analysis.Compounds (1) and (2) are isostructural and isomorphous with their crystals are monoclinic, space group P21/n, with Z=4.R=0.087 for 2 670 observed =3.0> reflections for (1) and 0.050 for 3525 observed reflections for (2) respectively.A similar reaction with a sigle-crystal X-ray diffraction study, is similar to that in
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Doi:10.1007/BF00955841
(1987)Doi:10.1021/acs.joc.9b01913
(2020)Doi:10.1021/jo8021633
(2009)Doi:10.1039/jr9570004510
(1957)Doi:10.1021/jo01065a091
(1961)Doi:10.1021/ja01469a026
(1961)
