Synlett (2014)
Update date:2022-08-03
Topics: Oxidative Addition Reductive Elimination Transmetalation
Baralle, Alexandre
Otsuka, Shinya
Guérin, Vincent
Murakami, Kei
Yorimitsu, Hideki
Osuka, Atsuhiro
NiCl2(PPh3)(IPr) catalyzes cross-coupling reactions of 2-methylsulfanylbenzofurans with alkyl Grignard reagents. Other nickel complexes such as NiCl2(dppe) failed to catalyze the same reaction. The alkylation is applicable to the synthesis of a couple of protein tyrosine phosphatase inhibitors, 3-(4-biphenylyl)-2-alkylbenzofurans.
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(2014)
