Chemistry Letters p. 1283 - 1286 (1987)
Update date:2022-08-05
Topics:
Hayashi, Masaji
Mukaiyama, Teruaki
In the presence of a catalytic amount of stannous halide, silyl enol ethers react with bromomethyl methyl ether to give the corresponding α-bromoethyl ketones, which are smoothly converted to α-methylenated ketones on the successive addition of tertiary amine by one-pot procedure.This method is successfully applied to a synthesis of sarkomycin intermediate.
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Doi:10.1021/jo00244a010
(1988)Doi:10.1016/S0040-4039(00)95918-5
(1987)Doi:10.1246/bcsj.60.3431
(1987)Doi:10.1002/chem.200801148
(2009)Doi:10.1071/CH11034
(2011)Doi:10.1016/S0040-4020(01)81664-1
(1987)
