Synthesis p. 900 - 902 (1988)
Update date:2022-08-04
Topics:
Guy, Alain
Lemor, Alain
Doussot, Joel
Lemaire, Marc
The benzylic proton of alkylarenes 1 was replaced by an azido group in one step by reaction with trimethylsilyl azide or hydrazoic acid in chloroform in the presence of 2,3-dichloro-5,6-dicyano-1,4-benzoquinone (DDQ).The 1-arylalkyl azides 2 were reduced to amines 3, which were characterized as their hydrochlorides 4.
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