Synthesis p. 978 - 979 (1988)
Update date:2022-08-05
Topics:
Berry, Nicola M.
Casy, Guy
Harwood, Laurence M.
Low temperature generation of dianions of 2-alkylated derivatives of dimedone, followed by alkylation at C-4 and quenching of the reaction mixture with acetic anhydride at room temperature furnishes the least sterically hindered 2,6-dialkyl-3-acetoxy-5,5-dimethyl-2-cyclohexenones 2 with high selectivity in a one-pot process.
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