SYNTHESIS OF TRINITROAROMATICS
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REFERENCES
1. Agrawal, J. P.; Hodgson, R. D. Organic Chemistry of Explosives; John Wiley & Sons Ltd.:
West Sussex, 2007; and references therein.
2. Albright, L. F.; Hanson, C. Industrial and Laboratory Nitrations (ACS Symposium Series
22); American Chemical Society: Washington, DC, 1976; (a) Ross, D. S.; Kirshen, N. A.
Chapter 7, 114–131; (b) Hanson, C.; Kaghazchi, T.; Pratt, M. W. T. Chapter 8, 132–155;
(c) Deno, N. C. Chapter 9, 156–159.
3. Olah, G. A.; Narang, S. C.; Olah, J. A.; Lammertsma, K. Recent aspects of nitration: New
preparative methods and mechanistic studies (a review). Proc. Natl. Acad. Sci. USA 1982,
79, 4487–4494.
4. Olah, G. A.; Malhotra, R.; Narang, S. C. Nitration: Methods and Mechanisms; VCH:
New York, 1989.
´
5. Urbanski, T. Chemistry and Technology of Explosives; Pergamon Press: New York, 1964;
(a) vol. 1 and (b) vol. 3; and references therein.
6. Kaufmann, A.; Decker, H. Ueber die nitrirung des chinolins und seiner mononitroderivate.
Studien in der chinolinreihe. II. Mittheilung. Ber. Dtsch. Chem. Ges. 1906, 39, 3648–3651.
7. Hill, M. E.; Taylor, Jr., F. Nitration of 1,3,5-trihalobenzenes. J. Org. Chem. 1960, 25,
1037–1038.
8. Dacons, J. C.; Taylor, Jr., F. Nitration of 1,3-dibromobenzene. J. Chem. Eng. Data. 1969,
14(4), 499–500.
9. Lu, L.; Ou, Y.; Wang, J. Synthesis of hexanitrohexaazaisowurtzitane by nitration with
super acids. Jingxi Huagong. 2004, 21(5), 321–323.
10. Lauer, K.; Oda, R. Konstitution und reaktionsfa¨higkeit, XV: Mitteilung: Reaktionskine-
tische untersuchung der nitrierung aromatischer verbindungen in schwefelsa¨ure. J. Prakt.
Chem. 1936, 144, 176–192.
11. Mehilal; Sikder, N.; Sikder, A. K.; Survase, D. V.; Agrawal, J. P. Studies on 2,4,6-
trinitrophloroglucinol (TNPG), a novel flash sensitizer. Ind. J. Eng. Mater. Sci. 2004,
11, 59–62.
12. Bellamy, A. J.; Ward, S. J.; Golding, P. A new synthetic route to 1,3,5-triamino-2,4,6-
trinitrobenzene (TATB). Propellants, Explos., Pyrotech. 2002, 27, 49–58.
13. Bellamy, A. J.; Golding, P.; Ward, S. J. Synthesis of 1,3,5-triamino-2,4,6-trinitrobenzene
(TATB) and diamino-2,4,6-trinitrobenzene (DATB). UK Patent GB 2,355,715 B, March
17, 2004.
14. Mitchell, A. R.; Coburn, M. D.; Lee, G. S.; Schmidt, R. D.; Pagoria, P. F.; Hsu, P. C.
Synthesis of trinitrophloroglucinol and triaminotrinitrobenzene (TATB). US Patent
7,057,073 B2, June 6, 2006.
15. DeFusco, A. A.; Nielsen, A. T.; Atkins, R. L. An improved preparation of trinitrophlor-
oglucinol. Org. Prep. Proced. Int. 1982, 14(6), 393–395.
16. DeFusco, Jr., A. A.; Nielsen, A. T.; Atkins, R. L. Synthesis of trinitrophloroglucinol.
US Patent 4,434,304, February 28, 1984.
17. Salter, D. A.; Simkins, R. J. J. Preparation of nitrophenols. US Patent 3,933,926, January
20, 1976.
18. Jackson, C. L.; Warren, W. H. The reactions of sodic alcoholates with tribromtrinitro-
benzol. Am. Chem. J. 1893, 15, 607–642.
´
´
´
19. Blanksma, J. J. Sur le tetranitrophenol, le pentanitrophenol et la pentanitrophenylnitra-
´
mine. Rec. Trav. Chim. 1902, 21, 254–268.
¨
20. Schlubach, H. H.; Mergenthaler, F. Uber die mono- und dimethoxy-pikrinsa¨uren und ihre
chloride. Ber. Dtsch. Chem. Ges. 1925, 58(12), 2732–2736.
21. Bellamy, A. J.; Golding, P.; Ward, S. J.; Mitchell, N. W. Nitration of 1,3,5-trimethoxy-
benzene. J. Chem. Res., Miniprint 2002, 0919–0930.