Bulletin of the Academy of Sciences of the USSR Division of Chemical Science p. 1739 - 1744 (1989)
Update date:2022-08-05
Topics:
Kozitsyna, N. Yu.
Surazhskaya, M. D.
Larina, T. B.
Koz'min, P. A.
Kotel'nikova, A. S.
Moiseev, I. I.
Reaction of tetrachlorodiacetatodirhenium dihydrate with triphenylphosphineplatinum(II) triacetatoargentate(I) produces a new binuclear platinum complex with acetate bridges, bis<(μ2-acetato)acetatotriphenylphosphine>diplatinum(II).The new complex is characterized by x-ray structural analysis, IR, and PMR spectrocopies.The Re(III) complex in this reaction is not only the source of chloride ions, which are necessary for precipitation of silver, and the acetate acceptor, but also the silver(I) reductant which is oxidized during the reaction to Re(IV).
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