STEREOSELECTIVE RADICAL CYCLIZATION FOR THE SYNTHESIS OF BICYCLIC HIGHER-CARBON SUGARS. SYNTHESIS OF THE SUGAR MOIETY OF OCTOSYL ACIDS

DOI: 10.1016/S0040-4039(00)99136-6

Source and publish data:

Tetrahedron Letters p. 2829 - 2832 (1989)

Update date:2022-09-26

Topics:

Authors:

Araki, Younosuke

Endo, Tadatoshi

Arai, Yoshifusa

Tanji, Masaki

Ishido, Yoshiharu

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Article abstract of DOI:10.1016/S0040-4039(00)99136-6

The Bu3SnH-AIBN induced radical cyclisation of 6-bromo-6-deoxy-3-O-<(E)-2-ethoxycarbonylethenyl>-1,2-O-isopropylidene-α-D-allofuranose (1) gave ethyl 3,7-anhydro-6,8-dideoxy-1,2-O-isopropylidene-α-D-glycero-D-allo-nonofuranuronate (2) in 80 percent yield.

Full text of DOI:10.1016/S0040-4039(00)99136-6

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