PREPARATION OF β-KETOMACROLACTONES AND β-KETODIOLIDES USING S-t-BUTYL 3-OXOBUTANETHIOATE AND S-t-BUTYL 4-DIETHYLPHOSPHONO-3-OXOBUTANETHIOATE

DOI: 10.1016/S0040-4020(01)89218-8

Source and publish data:

Tetrahedron p. 7565 - 7580 (1989)

Update date:2022-08-02

Topics: Preparation Experimental

Authors:

Booth, Paul M.

Broughton, Howard B.

Ford, Mark J.

Fox, Christina M. J.

Ley, Steven V.

et al. et al.

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Article abstract of DOI:10.1016/S0040-4020(01)89218-8

Using S-t-butyl 3-oxobutanethioate (1) and S-t-butyl 4-diethylphosphono-3-oxobutanethioate (2) various homologation reactions with t-butyldimethylsilyl protected hydroxy-iodides and aldehydes are reported.The products of these reactions after deprotection

Full text of DOI:10.1016/S0040-4020(01)89218-8

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Product name:S-t-butyl 12-triphenylmethyloxy-11-benzyloxy-3-oxododecanethioate

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