Synthesis p. 1083 - 1086 (1994)
Update date:2022-07-30
Topics:
Watanabe
Morimoto
Tomoda
Iwanaga
The Wittig-Horner reaction of dimethyl phthalide-3-phosphonates with various ketones was investigated under the conditions: lithium bis(trimethylsilyl)amide (LHMDS) or sodium hydride in tetrahydrofuran, and cesium carbonate in isopropyl alcohol. The sequential treatment of the 3-ylidenephthalides with diisobutylaluminium hydride (DIBAL-H) and pyridinium dichromate (PDC) afforded 2,2-disubstituted indan-1,3-dione derivatives in modest to high overall yields.
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Doi:10.1021/jo2001897
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(2012)Doi:10.1055/s-1990-26825
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(2015)Doi:10.1134/S1070428011010076
(2011)Doi:10.1080/00397911.2010.518272
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