Tetrahedron Asymmetry p. 605 - 608 (1993)
Update date:2022-08-03
Topics:
Tanaka
Itoh
Mitsuhashi
Maruno
Wakamatsu
The total synthesis of isoschizandrin 1 having the natural configuration was accomplished confirming the structure of 1 in unambiguous manner. Starting from optically pure 9, allylic alcohol 11 was obtained in good yield, and was then converted into epoxide 12 stereoselectively. Finally, reductive C-O bond fission afforded the natural enantiomer of isoschizandrin 1.
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