Journal of Organic Chemistry p. 3097 - 3102 (1991)
Update date:2022-08-02
Topics:
Berkowitz, William F.
Wilson, Phyllis J.
The preparation and free-radical bicyclic ring closure of 4-(2-bromo-2-propen-1-yl)cyclohexene 7 is described.The bicyclo<3.2.1> and -<2.2.2> alcohols 9 and 10 arising, respectively, from 5-exo and 6-endo (or 6-exo) modes of cyclization of a vinyl radical were isolated in a 1:1 ratio.Factors affecting the regiochemical outcome were investigated.
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