Tetrahedron Letters p. 1295 - 1298 (1991)
Update date:2022-08-03
Topics:
Adam, Waldemar
Hadjarapoglou, Lazaros
Wang, Xiaoheng
Various enol-type alkenes, such as 2,3-dimethylbenzodioxin (1), O-tetrabenzyl glycal (3), 1,2-bis(trimethylsilyloxy)cycloalkenes (9) were transformed in excellent yields to their labile epoxides by dimethyldioxirane (as acetone solution); the silyl ketene acetal 5 and 2-methyl-3-trimethylsilyloxybenzo[b]furan (7) gave the corresponding epoxide rearrangement products.
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