Synthesis of optically active nucleoside analogs containing 2,3- dideoxyapiose in the presence of a catalytic amount of trimethylsilyl iodide

DOI: 10.1248/cpb.41.1906

Source and publish data:

Chemical and Pharmaceutical Bulletin p. 1906 - 1909 (1993)

Update date:2022-08-02

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Authors:

Ohsawa Ohsawa

Shiozawa

Achiwa Achiwa

Terao Terao

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Article abstract of DOI:10.1248/cpb.41.1906

Optically pure (R)-4,4-diethoxy-2-(hydroxymethyl)butyl acetate (1) was synthesized enantioselectively by lipase-catalyzed transesterification from 4,4-diethoxy-2-(hydroxymethyl)butanol. Coupling of silylated nucleobases and 2-O-acetyl-5-O-pivaloyl-(3S)-2,

Full text of DOI:10.1248/cpb.41.1906

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